タイトル

開講年度 開講学部等
2025 工学部
開講学期 曜日時限 授業形態 AL(アクティブ・ラーニング)ポイント
後期 金5~6 講義 10.0
時間割番号 科目名[英文名] 使用言語 単位数
1062330950 機器分析Ⅱ[Instrumental AnalysisⅡ] 日本語 2
担当教員(責任)[ローマ字表記] メディア授業
山吹 一大[YAMABUKI Kazuhiro]
担当教員[ローマ字表記]
山吹 一大 [YAMABUKI Kazuhiro]
特定科目区分   対象学生   対象年次 3~
ディプロマ・ポリシーに関わる項目 カリキュラムマップ(授業科目とDPとの対応関係はこちらから閲覧できます)
授業の目的と概要
In this lecture, you will learn the basic outlines and principles of highly versatile analytical instruments used in these fields from faculty members who specialize in organic chemistry and polymer chemistry. In addition, you will deepen your understanding of instrumental analysis by knowing specific examples of measurements using the instrumental analysis and by imagining various actual measurement scenes through assignments. You will also take a tour of the actual equipment to ensure that your knowledge is firmly established. Furthermore, you will learn how and where the measuring devices you learned in the lectures are actually used in society.(DP3,5)
授業の到達目標
(1) Understand the principles and characteristics of each analytical instrument, and be able to interpret the results (spectra, numerical data, etc.) to derive conclusions from them.
(2) Be able to select the appropriate instrument for obtaining the information needed in different scenarios.
(3) Be able to propose comprehensive analyses by combining multiple analytical instruments.
(4) Reflect on the connection between the analytical instruments learned in the lectures and social issues, and appreciate the importance and necessity of chemical (scientific) analysis.
(5) Through group work and exercises related to analytical instruments, actively listen to the opinions of others and engage in spontaneous and proactive discussions.
(6) By observing the instruments and measurements learned in this lecture, be able to understand the entire process, from data preparation to measurement and analysis.
(7) Develop presentation skills by researching and presenting on the practical applications of the instruments covered in this lecture.
授業計画
【全体】
・Introduction of analyzers that are often used in general organic chemistry.
・The explanation will be as easy to understand as possible, and guidance will be provided so that students can propose their own analysis methods and results.
・Aim for an interactive lecture that emphasizes imagination rather than memorization.
・The first half will focus on classroom lectures, and the second half will include observations of instrumental analysis equipment, exercises, and group work.
・This lecture will be based on the following aspects of organic matter.

1. Surface observation

2. Chromatography (separation)

3. Thermal analysis

4. Spectroscopy

5. Practical exercises (equipment tours, exercises, group work)
項目 内容 授業時間外学習 備考
第1回 guidance Explain the flow of all lectures. Preparation/Review (Approximate study time: 4 hours or more)
第2回 SEM/TEM measurement Learn about the principles and uses of electron microscopes. Preparation/Review (Approximate study time: 4 hours or more)
第3回 AFM/STM measurement Learn about the principles and uses of microscopes that enable observation at the nano level. Preparation/Review (Approximate study time: 4 hours or more)
第4回 IR measurement Learn about the principles and applications of molecular structure analysis using infrared ray. Preparation/Review (Approximate study time: 4 hours or more)
第5回 XRD/XPS measurement Learn the principles and applications of molecular structure analysis using X-ray irradiation. Preparation/Review (Approximate study time: 4 hours or more)
第6回 GC/LC/GPC measurement Learn about separation mechanisms and applications in separation and purification methods for samples in gases and liquids. Preparation/Review (Approximate study time: 4 hours or more)
第7回 MS measurement Learn about the principles and applications of mass measurement using ionization of substances. Preparation/Review (Approximate study time: 4 hours or more)
第8回 UV/PL measurement Learn the principles and applications of structural analysis methods using light in the ultraviolet region. Preparation/Review (Approximate study time: 4 hours or more)
第9回 NMR(1) Learn about molecular structure analysis methods that utilize the interaction of nuclei of molecules placed in a magnetic field with electromagnetic wave. Preparation/Review (Approximate study time: 4 hours or more)
第10回 Fieldwork (equipment tour) Observing the equipment learned in the lecture, and confirming its operation method, scale, and data. Preparation/Review (Approximate study time: 4 hours or more)
第11回 General practice 1 Exercises related to instrumental analysis explained in previous lectures will be conducted. (individual) Preparation/Review (Approximate study time: 4 hours or more)
第12回 group work 1 Disseminate information using the instrumental analysis explained in the lectures so far. (group) Preparation/Review (Approximate study time: 4 hours or more)
第13回 group work 2 Disseminate information using the instrumental analysis explained in the lectures so far. (group) Preparation/Review (Approximate study time: 4 hours or more)
第14回 group work 3 Disseminate information using the instrumental analysis explained in the lectures so far. (group) Preparation/Review (Approximate study time: 4 hours or more)
第15回 General practice 2 Comprehensive exercises and commentary on the instrumental analysis explained in the previous lectures will be given. Preparation/Review (Approximate study time: 4 hours or more)
※AL(アクティブ・ラーニング)欄に関する注
・授業全体で、AL(アクティブ・ラーニング)が占める時間の割合を、それぞれの項目ごとに示しています。
・A〜Dのアルファベットは、以下の学修形態を指しています。
【A:グループワーク】、【B:ディスカッション・ディベート】、【C:フィールドワーク(実験・実習、演習を含む)】、【D:プレゼンテーション】
A: 30% B: 20% C: 30% D: 20%
成績評価法
Assessment will be based on a combination of in-class quizzes, out-of-class assignments (reports), presentations, and a final written exam.
(Mini quizzes 5%, Out-of-class assignments 10%, Presentations 15%, Final written exam 70%)
教科書にかかわる情報
備考
Distribution print available
参考書にかかわる情報
備考
Not specified. The library has many easy-to-understand reference books on instrumental analysis. Please make your own selections to deepen your understanding of the lectures.
メッセージ
In this lecture, we will provide a general overview of analytical instruments that can be used in organic chemistry. The key focus is on "understanding what can be determined using these instruments." Once this is understood, it will enable efficient analysis methods in both laboratory experiments and real-world work settings. In addition to the lecture, we will also work through individual and group exercises to help you gain knowledge about each analytical instrument.
キーワード
organic chemistry, instrumental analysis
持続可能な開発目標(SDGs)

  • 安全な水とトイレをみんなに
  • エネルギーをみんなに そしてクリーンに
  • つくる責任つかう責任
  • 気候変動に具体的な対策を
  • 海の豊かさを守ろう
  • Life on land
(水・衛生)すべての人々の水と衛生の利用可能性と持続可能な管理を確保する。
(エネルギー)すべての人々の、安価かつ信頼できる持続可能な近代的エネルギーへのアクセスを確保する。
(持続可能な生産と消費)持続可能な生産消費形態を確保する。
(気候変動)気候変動及びその影響を軽減するための緊急対策を講じる。
(海洋資源)持続可能な開発のために海洋・海洋資源を保全し、持続可能な形で利用する。
(陸上資源)陸域生態系の保護、回復、持続可能な利用の推進、持続可能な森林の経営、砂漠化への対処、ならびに土地の劣化の阻止・回復及び生物多様性の損失を阻止する。
関連科目
General lectures related to organic chemistry and polymer chemistry, Applied Chemistry Experiment III
履修条件
連絡先
Kazuhiro Yamabuki
Email: yamabuki@yamaguchi-u.ac.jp
オフィスアワー
I am available any time I have free time.

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